9000 Series Methods

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Table of Contents

Method 9000 (PDF) (12 pp, 46K)
Determination of Water in Waste Materials by Karl Fischer Titration

Method 9001 (PDF) (10 pp, 42K)
Determination of Water in Waste Materials by Quantitative Calcium Hydride Reaction

Method 9010C (PDF) (10 pp, 58K)
Total and Amenable Cyanide: Distillation

Method 9012B (PDF) (13 pp, 100K)
Total and Amenable Cyanide (Automated Colorimetric, with Off-Line Distillation)

Method 9013 (PDF) (6 pp,157K)
Cyanide Extraction Procedure for Solids and Oils

Method 9014 (PDF) (7 pp, 72K)
Titrimetric and Manual Spectrophotometric Determinative Methods for Cyanide

Method 9020B (PDF) (13 pp, 190K)
Total Organic Halides (TOX)

Method 9021 (PDF) (12 pp, 197K)
Purgeable Organic Halides (POX)

Method 9022 (PDF) (11 pp, 248K)
Total Organic Halides (TOX) by Neutron Activation Analysis

Method 9023 (PDF) (8 pp, 92K)
Extractable Organic Halides (EOX) in Solids

Method 9030B (PDF) (15 pp, 113K)
Acid-Soluble and Acid-Insoluble Sulfides: Distillation

Method 9031 (PDF) (16 pp, 316K)
Extractable Sulfides

Method 9034 (PDF) (7 pp, 60K)
Titrimetric Procedure for Acid-Soluble and Acid-Insoluble Sulfides

Method 9035 (PDF) (6 pp, 215K)
Sulfate (Colorimetric, Automated, Chloranilate)

Method 9036 (PDF) (7 pp, 225K)
Sulfate (Colorimetric, Automated, Methylthymol Blue, AA II)

Method 9038 (PDF) (6 pp, 186K)
Sulfate (Turbidimetric)

Method 9040C (PDF) (5 pp, 25K)
pH Electrometric Measurement

Method 9041A (PDF) (4 pp, 66K)
pH Paper Method

Method 9045D (PDF) (5 pp, 30K)
Soil and Waste pH

Method 9050A (PDF) (5 pp, 31K)
Specific Conductance

Method 9056A (PDF) (19 pp, 280K)
Determination of Inorganic Anions by Ion Chromatography

Method 9057 (PDF) (6 pp, 44K)
Determination of Chloride from HCl/Cl₂ Emission Sampling Train (Methods 0050 and 0051) by Anion Chromatography

Method 9060A (PDF) (5 pp, 26K)
Total Organic Carbon

Method 9065 (PDF) (7 pp, 212K)
Phenolics (Spectrophotometric, Manual 4-AAP with Distillation)

Method 9066 (PDF) (7 pp, 223K)
Phenolics (Colorimetric, Automated 4-AAP with Distillation)

Method 9067 (PDF) (7 pp, 160K)
Phenolics (Spectrophotometric, MBTH with Distillation)

Method 9070A (PDF) (1 pg, 16K)
See Method 1664, Publication No. EPA-821-R-98-002

Method 9071B (PDF) (13 pp, 82K)
n-Hexane Extractable Material (HEM) for Sludge, Sediment, and Solid Samples

Method 9074 (PDF) (15 pp, 85K)
Turbidimetric Screening Method for Total Recoverable Petroleum Hydrocarbons in Soil

Method 9075 (PDF) (7 pp, 62K)
Test Method for Total Chlorine in New and Used Petroleum Products by X-Ray Fluorescence Spectrometry (XRF)

Method 9076 (PDF) (10 pp, 81K)
Test Method for Total Chlorine in New and Used Petroleum Products by Oxidative Combustion and Microcoulometry

Method 9077 (PDF) (21 pp, 334K)
Test Methods for Total Chlorine in New and Used Petroleum Products (Field Test Kit Methods)

Method 9078 (PDF) (7 pp, 32K)
Screening Test Method for Polychlorinated Biphenyls in Soil

Method 9079 (PDF) (13 pp, 46K)
Screening Test Method for Polychlorinated Biphenyls in Transformer Oil

Method 9080 (PDF) (9 pp, 266K)
Cation-Exchange Capacity of Soils (Ammonium Acetate)

Method 9081 (PDF) (4 pp, 135K)
Cation-Exchange Capacity of Soils (Sodium Acetate)

Method 9090A (PDF) (16 pp, 611K)
Compatibility Test for Wastes and Membrane Liners

Method 9095B (PDF) (4 pp, 28K)
Paint Filter Liquids Test

Method 9096 (PDF) (14 pp, 249K)
Liquid Release Test (LRT) Procedure

Method 9100 (PDF) (57 pp, 866K)
Saturated Hydraulic Conductivity, Saturated Leachate Conductivity, and Intrinsic Permeability

Method 9131 (PDF) (18 pp, 301K)
Total Coliform: Multiple Tube Fermentation Technique

Method 9132 (PDF) (13 pp, 236K)
Total Coliform: Membrane-Filter Technique

Method 9210A (PDF) (12 pp, 122K)
Potentiometric Determination of Nitrate in Aqueous Samples with Ion-Selective Electrode

Method 9211 (PDF) (8 pp, 68K)
Potentiometric Determination of Bromide in Aqueous Samples with Ion-Selective Electrode

Method 9212 (PDF) (8 pp, 69K)
Potentiometric Determination of Chloride in Aqueous Samples with Ion-Selective Electrode

Method 9213 (PDF) (8 pp, 65K)
Potentiometric Determination of Cyanide in Aqueous Samples and Distillates with Ion-Selective Electrode

Method 9214 (PDF) (8 pp, 68K)
Potentiometric Determination of Fluoride in Aqueous Samples with Ion-Selective Electrode

Method 9215 (PDF) (9 pp, 66K)
Potentiometric Determination of Sulfide in Aqueous Samples and Distillates with Ion-Selective Electrode

Method 9216 (PDF) (13 pp, 126K)
Potentiometric Determination of Nitrite in Aqueous Samples with Ion-Selective Electrode

Method 9250 (PDF) (5 pp, 206K)
Chloride (Colorimetric, Automated Ferricyanide AAI)

Method 9251 (PDF) (5 pp, 204K)
Chloride (Colorimetric, Automated Ferricyanide AAII)

Method 9253 (PDF) (6 pp, 140K)
Chloride (Titrimetric, Silver Nitrate)

Method 9310 (PDF) (9 pp, 165K)
Gross Alpha and Gross Beta

Method 9315 (PDF) (7 pp, 202K)
Alpha-Emitting Radium Isotopes

Method 9320 (PDF) (10 pp, 267K)
Radium-228

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9000 Series Methods

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